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Syntheses of Three New Pyridyl Thienopyridine Ligands via the Hurtley Reaction
Mälardalen University, School of Sustainable Development of Society and Technology.
Mälardalen University, School of Sustainable Development of Society and Technology.
Mälardalen University, School of Sustainable Development of Society and Technology.
2012 (English)In: Journal of Heterocyclic Chemistry, ISSN 0022-152X, E-ISSN 1943-5193, Vol. 49, no 6, p. 1290-1295Article in journal (Refereed) Published
Abstract [en]

The tridentate pyridyl thienopyridines 5-phenyl-7-(pyridin-2-yl)thieno[2,3-c]pyridine (L1), 7-(pyridin-2-yl)-5-(thiophen-2-yl)-thieno[2,3-c]pyridine (L2) and 5,7-di(pyridin-2-yl)thieno[2,3-c]pyridine (L3) have been synthesized via the Hurtley reaction. L1 and L2 were synthesized by condensing 3-bromothiophene-2-carboxylic acid with phenyl-1,3-butanedione and 1-thienyl-1,3-butanedione respectively. L3 was synthesized by condensing 3-bromothiophene-2-carboxylic acid with benzoylacetonitrile. Ring closure and a subsequent Negishi or Stille cross-coupling afforded L1, L2, and L3 in an overall yield of 20, 3, and 6%, respectively.

Place, publisher, year, edition, pages
2012. Vol. 49, no 6, p. 1290-1295
National Category
Natural Sciences
Identifiers
URN: urn:nbn:se:mdh:diva-17704DOI: 10.1002/jhet.903ISI: 000312298300002Scopus ID: 2-s2.0-84870936683OAI: oai:DiVA.org:mdh-17704DiVA, id: diva2:588339
Available from: 2013-01-15 Created: 2013-01-15 Last updated: 2018-01-03Bibliographically approved

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Steen, Robert O.Nurkkala, Lasse J.Dunne, Simon J.
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